cosio_d20

Fit result

Overall status	Success
time	0.022 s
iterations	3
reduced χ²	4.45
Rwp	3.97 %
Rwp, d20	3.97 %

Fitted parameters

#	datablock	category	entry	parameter	units	start	value	s.u.	change
1	cosio	cell		length_a	Å	10.3088	10.3087	0.0003
2	cosio	cell		length_b	Å	6.0038	6.00379	0.00015
3	cosio	cell		length_c	Å	4.78667	4.78665	0.00012
4	cosio	atom_site	Co1	adp_iso	Å²	0.276007	0.66	0.11	140.7% ↑
5	cosio	atom_site	Co2	fract_x		0.279306	0.2792	0.0008
6	cosio	atom_site	Co2	fract_z		0.984747	0.9847	0.0015
7	cosio	atom_site	Si	fract_x		0.0937956	0.0940	0.0004	0.2% ↑
8	cosio	atom_site	Si	fract_z		0.42903	0.4294	0.0009	0.1% ↑
9	cosio	atom_site	Si	adp_iso	Å²	0.345845	0.67	0.09	92.4% ↑
10	cosio	atom_site	O1	fract_x		0.0910597	0.0911	0.0003
11	cosio	atom_site	O1	fract_z		0.771383	0.7715	0.0007
12	cosio	atom_site	O1	occupancy		1	0.916	0.014	8.4% ↓
13	cosio	atom_site	O1	adp_iso	Å²	0.646232	0.46	0.08	29.0% ↓
14	cosio	atom_site	O2	fract_x		0.448228	0.4481	0.0003
15	cosio	atom_site	O2	fract_z		0.216607	0.2169	0.0007	0.1% ↑
16	cosio	atom_site	O2	occupancy		1	0.959	0.014	4.1% ↓
17	cosio	atom_site	O2	adp_iso	Å²	0.578425	0.66	0.09	14.2% ↑
18	cosio	atom_site	O3	fract_x		0.16354	0.1636	0.0003
19	cosio	atom_site	O3	fract_y		0.0316621	0.0315	0.0004	0.4% ↓
20	cosio	atom_site	O3	fract_z		0.280034	0.2801	0.0005
21	cosio	atom_site	O3	occupancy		1	0.954	0.012	4.6% ↓
22	cosio	atom_site	O3	adp_iso	Å²	0.834654	0.84	0.07	1.2% ↑
23	d20	peak		broad_gauss_u	deg²	0.242221	0.241	0.007	0.6% ↓
24	d20	peak		broad_gauss_v	deg²	-0.528471	-0.527	0.015	0.2% ↑
25	d20	peak		broad_gauss_w	deg²	0.383635	0.385	0.009	0.5% ↑
26	d20	peak		broad_lorentz_y	deg	0.0161112	0.015	0.005	8.6% ↓
27	d20	instrument		calib_twotheta_offset	deg	0.286095	0.286	0.002	0.1% ↓
28	d20	linked_structure	cosio	scale		1.19516	1.33	0.03	11.1% ↑
29	d20	background	1	intensity		609.315	609	15
30	d20	background	2	intensity		581.182	581	10
31	d20	background	3	intensity		563.371	563	10
32	d20	background	4	intensity		540.696	541	9
33	d20	background	5	intensity		520.194	520	6
34	d20	background	6	intensity		507.647	508	4
35	d20	background	7	intensity		463.241	463	4	0.1% ↓
36	d20	background	8	intensity		434.379	431	3	0.8% ↓
37	d20	background	9	intensity		450.935	452	3	0.1% ↑
38	d20	background	10	intensity		430.455	429	3	0.3% ↓
39	d20	background	11	intensity		413.876	414	3	0.1% ↓
40	d20	background	12	intensity		361.288	362	3	0.2% ↑
41	d20	background	13	intensity		290.81	293	2	0.6% ↑
42	d20	background	14	intensity		238.517	241	3	0.9% ↑

startthe value before the fit
valuethe fitted value
s.u.its standard uncertainty
changehow far the fit moved it, in % of the start: ↑ up, ↓ down